Instruments Handled: HPLC and LC-MS (Agilent, Shimadzu, Hitachi with UV & PDA) GC and GC-MS (Agilent, Shimadzu - Head space) ICP-MS (Agilent) UV - Vis Spectrophotometer (Shimadzu UV 1700, Elico LI – 127) FTIR (Agilent, Shimadzu-8400S) Karl Fisher Titrator (Metrohm) Autotitrator (Metrohm785DMP) DSC and Particle size (Metrohm)Job Responsibilities:• To lead and execute the analytical Team for method development, Validation and structure elucidation activities on HPLC/LC-MS, GC/GC-MS and routine analysis of analytical laboratory.• To calibrate and validate the method as per standards• Responsible for calibration & trouble shooting of Analytical instruments i.e. HPLC, LC-MS, GC, GCMS, IR, UV, Karl Fisher as per master calibration schedule• Analytical method development and Validation using instruments HPLC & GC.• Preparation and review of specification, method of analysis procedure, COA, SOP, technical documents and reports, Method Validation Protocol, validation reports, method transfer protocols, • Monitoring of routine Analytical functions like in-process & finished product.• Technical Assessments of projects (screening, pipeline and development project stages and literature search) • Force Degradation study and stress Stability Study as per ICH guidelines.• Determination of Residual solvents by GC headspace.• Preparation and Standardization of Volumetric Solutions, Reagents and Indicators• Storage & Qualification of Reference standards, working standards and impurities,• Assisting in establishment of lab for NABL Accreditation (ISO/IEC 17025:2017).• Responsible for Lab safety, GLP, 5S and its documentation & to maintain experimental data in LIMS/ PV.

API & Pharmaceutical Intermediates manufacturing company. Instruments Handled :HPLC (Agilent, Shimadzu, Hitachi with UV, PDA & RI Detector)GC (Shimadzu 2010 & 5000 - Head space)UV - Vis Spectrophotometer (Shimadzu UV 1700, Elico LI – 127)FTIR (Shimadzu-8400S)pH – METER (Elico & Lab India)Karl Fisher Titrator (Metrohm)Polarimeter (Perkin Elmer -341)Autotitrator (Metrohm785DMP)Job Responsibilities :Managing the daily activities of Analytical laboratory.Responsible for calibration & trouble shooting of instruments GC, HPLC, IR, UV, Karl Fisher, DSC and SOR (Polarimeter). Analytical method development and Validation using instruments GC and HPLC.Monitoring of routine Analytical functions like in-process control & finished product by using analytical instruments.Force Degradation study and stress Stability Study as per ICH guidelines.Determination of Residual solvents in finished products by GC headspace.Chiral separation of racemates by employing analytical instruments Preparation and Standardization of Volumetric Solutions, Reagents and IndicatorsPreparation of COA, Protocol and Reports of Finish products.Preparation and maintaining the Working standard and primary standard.