Melissa Willoughby Email and Phone Number

Sampling and testing incoming raw materials for release to be used in commercial manufacturing.

Prepped and analyzed drinking water and waste water samples by EPA GC Mas Spec VOA methods 524.2, 8260B and 624.1. Back up analysts for the preparation and analyses of drinking water and waste water samples by EPA GC Pesticide, PCB and Herbicide methods 8081A, 8151A, 608, 504, 508, 515.1, 548.1 and 552.1.Prepared data packets for all samples analyzedPerform routine instrument and autosampler maintenanceWrite and updated Standard Operating Procedures (SOPs)Performed peer review of; analytical, standard prep and sample prep notebooks, raw data and analytical data packetPoint of contact for all internal and external audits

GC Mas Spec Analyst (February 2004 - June 2006)Prepped and analyzed drinking water, waste water and soil samples by EPA GC Mas Spec VOA methods 524.2, 8260B and 624.1. Prepped and analyzed waste water and soil samples by EPA GC/VOA 8015B and 8021. Back up analysts for the preparation and analyses of drinking water and waste water samples by EPA GC Pesticide, PCB and Herbicide methods 8081A, 8151A, 608, 504, 508, 515.1, 548.1 and 552.1.Prepared data packets for all samples analyzedPerform routine instrument and autosampler maintenanceWrite and updated Standard Operating Procedures (SOPs)Help cross train and train new analyst on GC methods and sample prepPerformed peer review of; analytical notebooks, standard prep, sample prep, raw data and analytical data packetPoint of contact for all internal and external audits GC Team Leader (February 2003 - February 2004)Coordinated instrumentation time and personal for the analysis of samples. Prepped and analyzed drinking water, waste water and soil samples by; EPA GC/ECD Pesticide, PCB, CPMA/DCMA and Herbicide methods 8081A, 8151A, 608, 504, 508, 515.1, 548.1 and DCMA; EPA GC/FID TPH and Diesel methods 8015B; and Air samples for Solvents and PCBs by NIOSH methodology.Prepared data packets for samples analyzedPerformed peer review of all analytical, standard prep and sample prep notebooks, raw data and analytical data packet generated by the GC analysis groupPerform routine instrument and autosampler maintenanceAnalytical method development Sample prep method development.Training of all new GC analyst on analysis and sample prepWrite and updated Standard Operating Procedures (SOPs)Subject Matter Expert (SME) and point of contact for all internal and external audits

GC Group Leader (February 2002 - February 2003)Prepped and analyzed drinking water, waste water and soil samples by; EPA GC/ECD Pesticide, PCB, CPMA/DCMA and Herbicide methods 8081A, 8151A, 608, 504, 508, 515.1, 548.1 and DCMA; EPA GC/FID TPH and Diesel methods 8015B; and Air samples for Solvents and PCBs by NIOSH methodology.Prepared data packets for samples analyzedPerformed peer review of all analytical, standard prep and sample prep notebooks, raw data and analytical data packet generated by the GC analysis groupPerform routine instrument and autosampler maintenanceAnalytical method development Sample prep method development.Training of all new GC analyst on analysis and sample prepWrite and updated Standard Operating Procedures (SOPs)Subject Matter Expert (SME) and point of contact for all internal and external audits

GC Group Leader ( October 1998 - February 2002 )Prepped and analyzed drinking water, waste water and soil samples by; EPA GC/ECD Pesticide, PCB, CPMA/DCMA and Herbicide methods 8081A, 8151A, 608, 504, 508, 515.1, 548.1 and DCMA; EPA GC/FID TPH and Diesel methods 8015B; and Air samples for Solvents and PCBs by NIOSH methodology.Prepared data packets for all samples analyzedPerformed peer review of all analytical, standard prep and sample prep notebooks, raw data and analytical data packet generated by the GC analysis groupPerform routine instrument and autosampler maintenanceAnalytical method development Sample prep method developmentTraining of all new GC analyst on analysis and sample prepWrite and updated Standard Operating Procedures (SOPs)Subject Matter Expert (SME) and point of contact for all internal and external audits Setup and ran an on site lab in Saipan for the analysis of PCBs in soil by EPA 8082Chemist / Senior Chemist ( 1993 - October 1998 )Prepped and analyzed drinking water, waste water and soil samples by; EPA GC/ECD Pesticide, PCB, CPMA/DCMA and Herbicide methods 8081A, 8151A, 608, 504, 508, 515.1, 548.1 and DCMA; EPA GC/FID TPH and Diesel methods 8015B; and Air samples for Solvents and PCBs by NIOSH methodology.Prepared data packets for all samples analyzedPerformed peer review of all analytical notebooks, standard prep, sample prep, raw data and analytical data packet generated by the GC analysis groupPerform routine instrument and autosampler maintenanceAnalytical method development Sample prep method developmentWrite and updated Standard Operating Procedures (SOPs)Subject Matter Expert (SME) and point of contact for all internal and external audits Setup and ran an on site lab in Saipan for the analysis of PCBs in soil by EPA 8082Setup analytical equipment and trained analyst on equipment in Minsk, Belarus